Portable x-ray fluorescence for assessing trace elements in rice and rice products: Comparison with inductively coupled plasma-mass spectrometry

David E.B. Fleming, Kelly A. Foran, Jong Sung Kim, Judy R. Guernsey

Research output: Contribution to journalArticlepeer-review

27 Citations (Scopus)

Abstract

Portable x-ray fluorescence (XRF) was investigated as a means of assessing trace elements in rice and rice products. Using five measurement trials of 180. s real time, portable XRF was first used to detect arsenic (As), manganese (Mn), iron (Fe), nickel (Ni), copper (Cu), and zinc (Zn) in a variety of rice samples. The same samples were then microwave-digested and used to determine elemental concentrations using inductively coupled plasma-mass spectrometry (ICP-MS). The concentrations of As, Mn, Fe, Cu, and Zn determined by ICP-MS were found to be consistent with other recent studies involving various types of rice and rice products. When assessing for As, Mn, Fe, Cu, and Zn, comparison of results between XRF amplitude and ICP-MS concentration (wet weight) demonstrated a linear relationship with a significant correlation. A significant correlation between XRF amplitude and ICP-MS concentration was not found when assessing for Ni.

Original languageEnglish
Pages (from-to)217-223
Number of pages7
JournalApplied Radiation and Isotopes
Volume104
DOIs
Publication statusPublished - Oct 1 2015

Bibliographical note

Funding Information:
This work was supported by a Discovery Grant from the Natural Sciences and Engineering Research Council of Canada (Grant number: 261523 ). The project was supported with Pilot Study funding from the Atlantic RURAL Centre, enabled through the Canadian Institutes of Health Research (Grant number CDA-66534 ). The Health and Environments Research Centre (HERC) Laboratory was the recipient of major equipment funding through the Canadian Aerosol Research Network (CARN) from the Canada Foundation for Innovation. The authors thank Dr. Xiujuan (Kay) Yang for the ICP-MS analysis.

Publisher Copyright:
© 2015 Elsevier Ltd.

ASJC Scopus Subject Areas

  • Radiation

PubMed: MeSH publication types

  • Comparative Study
  • Evaluation Study
  • Journal Article
  • Research Support, Non-U.S. Gov't

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