A rotatable flat coil for static solid-state nuclear magnetic resonance spectroscopy

Jan K. Rainey; Jeffrey S. DeVries; Brian D. Sykes

doi:10.1063/1.1994899

A rotatable flat coil for static solid-state nuclear magnetic resonance spectroscopy

Jan K. Rainey, Jeffrey S. DeVries, Brian D. Sykes

Résultat de recherche: Article › examen par les pairs

5 Citations (Scopus)

Résumé

A holder allowing rotation of a flat coil relative to the static magnetic field (B₀) of a nuclear magnetic resonance (NMR) spectrometer over the range of orientations from parallel to perpendicular has been built and incorporated into a two-channel wide line static solid-state NMR probe. Radio frequency induction by the coil is perpendicular to B₀ for all rotational angles. Such a coil holder provides ready access to an additional directional variable for experiments exploiting sample orientation such as those using planar-supported oriented phospholipid bilayers. Rotation of the flat coil is demonstrated using ³¹P NMR of oriented phospholipid and peptide bilayers sandwiched between pairs of mica substrates.

Langue d'origine	English
Numéro d'article	086102
Pages (de-à)	1-4
Nombre de pages	4
Journal	Review of Scientific Instruments
Volume	76
Numéro de publication	8
DOI	https://doi.org/10.1063/1.1994899
Statut de publication	Published - août 2005
Publié à l'externe	Oui

Note bibliographique

Funding Information:
Thanks to Sam Graziano at the Faculty of Medicine Workshop for helpful discussions and expert machining and to Marc Genest in PENCE for peptide synthesis and purification. JKR is supported by Postdoctoral Fellowships from the Natural Sciences and Engineering Research Council of Canada and the Alberta Heritage Foundation for Medical Research. BDS receives support as a Canada Research Chair in Structural Biology. Funding is from the Canadian Protein Engineering Network of Centres of Excellence (PENCE).

ASJC Scopus Subject Areas

Instrumentation

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10.1063/1.1994899

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title = "A rotatable flat coil for static solid-state nuclear magnetic resonance spectroscopy",

abstract = "A holder allowing rotation of a flat coil relative to the static magnetic field (B0) of a nuclear magnetic resonance (NMR) spectrometer over the range of orientations from parallel to perpendicular has been built and incorporated into a two-channel wide line static solid-state NMR probe. Radio frequency induction by the coil is perpendicular to B0 for all rotational angles. Such a coil holder provides ready access to an additional directional variable for experiments exploiting sample orientation such as those using planar-supported oriented phospholipid bilayers. Rotation of the flat coil is demonstrated using 31P NMR of oriented phospholipid and peptide bilayers sandwiched between pairs of mica substrates.",

author = "Rainey, {Jan K.} and DeVries, {Jeffrey S.} and Sykes, {Brian D.}",

note = "Funding Information: Thanks to Sam Graziano at the Faculty of Medicine Workshop for helpful discussions and expert machining and to Marc Genest in PENCE for peptide synthesis and purification. JKR is supported by Postdoctoral Fellowships from the Natural Sciences and Engineering Research Council of Canada and the Alberta Heritage Foundation for Medical Research. BDS receives support as a Canada Research Chair in Structural Biology. Funding is from the Canadian Protein Engineering Network of Centres of Excellence (PENCE).",

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AU - DeVries, Jeffrey S.

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A rotatable flat coil for static solid-state nuclear magnetic resonance spectroscopy

Résumé

Note bibliographique

ASJC Scopus Subject Areas

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